12 JZS-Chem6 Revised Version

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Absorption stretching band were detected at 1679.66 cm-1 in FT- IR ... In the FT- IR spectrum of TAE-wall pistachio has a new ..... (2010). [3] William Kemp. ... Carbon prepared from Achyranthesaspera Linn. by X-ray fluorescence spectroscopy.

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Potential of Pistachio Pistachio-Hard Shell Based Thiosemicarbazone Acetophenone Thiosemicarbazone-Acetophenone for Pb2+Metal Sorption:: Kinetic Studies, Isotherms Modeling and Optimization Shameran Jamal Salih1 & Rezhna Hassan Faraj1 1 Faculty of Science and Health -Koya University, Koysinjaq KOY45, Erbil, Iraq E-mail: [email protected] koyauniversity.org

Article info

Abstract

Original: 21 August 2016 Revised: 10 October 2016 Accepted: 16 October 2016 Published online: 20 March 2017

The batch studies conducted in the present work provide significant information regarding the adsorption of Pb2+ onto Pistachio-Hard shell-grafted grafted-Thiosemicarbazone acetophenone. The sorption kinetics, isotherms and thermodynamics of Pb2+ onto acetophenone. adsorbent surface modified thiosemicarbazone acetophenone has been assessed under various operation conditions such as contact contact time, initial concentration of Pb2+, pH of the solution, temperature and adsorbent dosage. The FT-IR FT IR results of Pistachio-Hard shell grafted-Thiosemicarbazone hiosemicarbazone acetophenone showed that biomass has different functional groups and these functional groups are able to graft with Pb2+ in aqueous solution. The removal process reached maximum which was 97.08%. Equilibrium data fitted well with Freundlich isotherm model (1/n