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1HNMR spectra of BSPB diamines and IR spectra of resulting ...
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1HNMR spectra of BSPB diamines and IR spectra of resulting polyimide membranes. Fig. S2 IR spectra of NTDA-BSPB membranes. ppm. Fig. S1 1HNMR ...
HNMR spectra of BSPB diamines and IR spectra of resulting polyimide membranes
4
5
6
OCH2CH2CH2SO3H 2
3
1
H2 N
NH2 2
3
5
4
HO3SH2CH2CH2CO
3
6
1
4 overlapped 6
NH2
2
6
From Et3N
1
5
4
4
5
6
1
3
2
3
1
5
3
2
OCH2CH2CH2SO3H H2N
NH2 2
2
1
4 From Et3N
HO3SH2CH2CH2CO 6
5
4
NH2
3
overlapped
5
6
7
6
5
4
3
2
ppm Fig. S1 1HNMR spectra of BSPB diamine monomers.
3500
3000
2500
2000
1500
1035
NTDA-3,3'-BSPB
1712 1672
NTDA-2,2'-BSPB
1350 1201
2965
T/%
1
1000
-1
Wavenumber / cm
Fig. S2 IR spectra of NTDA-BSPB membranes.
500
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