research artides and reviews inthe field of natural volatiles and essential oils induding ... Published four times per year, NVEO provides artides on the aramatic ...
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ISEO 2014 Abstracts
Nat. Vol. Essent. Oils, Speciallssue
2014
NVEO
A Quarterly Open Access Scientific Journal
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Gökalp iscan
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Publisher: Badebio Ltd. Turkey
Scope NVEO is a major forum for the publication of new findings and research into natural volatiles and essential oils. It is created by the Permanent Scientific Committee of ISEO (International Symposium on Essential Oils). The journal is principally aimed at publishing proceedings of the ISEOs, but is alsa a peer reviewed journal for publishing original research artides and reviews in the field of natural volatiles and essential oils induding wide ranging related issues on the analysis, chemistry, biological and pharmacological activities, applications and regulatory affairs, etc. Published four times per year, NVEO provides artides on the aramatic principles of biological materials such as plants, animals, insects, microorganisms, in this field.
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NVEO
INTERNATIONAL 5YMP051UM
Natural Volatiles & Essential Oils
ON E55ENTIAL OlL5
07-10 September 2014. Istanbul
PP-074. The volatlles obtained from the gum and roots of Feru/a Joetida St.-lag. with conventlonal
and microscale techniques
Daniya T.AsiIbekova
1,
Gülmira Özek
l, Temel
Özek
2
Shahmansur
Sh. Sagdu/laev \ K.Hüsnü Can Baser
2
1 Acad. S.Yu.Yunusov Institute of the Chemistry of Plant Substances, Academy of Sciences of the Republic of 100170 Tashkent, Uzbekistan 1 Department of Pharmacognosy, Faculty of Pharmacy, Anadolu University, 26470 Eskisehir, Turkey
The objective of the present study was focused on the evaluation of chemical composition ofvolatiles and lipids from gum and roots of Ferula Joetida St.-lag. (Apiaceae). The gum and root were collected in Ojizzakh region (Republic of Uzbekistan) in 2013. The gum and roots of F.Joetida were subjected to hydrodistillation in Clevenger apparatus as well as Micro-Steam Distillation - Solid Phase Micro-Extraction (MSD-SPME) techniques to yield volatiles. Blue fiber with polydimethylsiloxane/ divinylbenzene adsorbent was applied for 3 min to extract volatiles from the gum and roots. Fatty acid's fraction of the gum and root was investigated after extraction by Folch method and subsequent saponification with 10% methanolic KOH. Fatty acids were partitioned by diethyl ether following acidification to pH 2, dried and converted to methyl esters using boron trifluoride-methanol solution. Ali the volatiles and fatty acid methyl esters were analyzed by GC/FIO and GC/MS techniques. Vields of volatiles
obtained
by Clevenger from gum and root were 7.5 and 0.53 ml% on dry weight,
respectively.
Ali the
volatiles were predominated with sulfur containing constituents like di-sec-butyl disulfide, trans-propenyl sec butyl disulfide, cis-propenyl sec butyl disulfide. One unknown sulfur containing constituent was detected in different amount in the gum as well as in the roots. The lipids extracted from the gum and roots were found to be rich with saturated palmitic, and unsaturated acids like oleic and linoleic.
ISEO
2014
Abstracts
Nat.
Vol. Essent.
Oils, Speciallssue
2014/125