Supplemental Information Platinum-decorated ... - Caltech Authors
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Figure S1. Schematic of the electrospray apparatus.1
Figure S2. TGA profiles of 30 (red) and 46 wt% (black) Pt-CNTs under a flow of air, Ar, and 2.04% H2 bal at 200 mL min-1 and a heating rate of 10 °C min-1. The negligible mass change (< 1%) upon switched from oxidizing to reducing atmosphere indicates there is negligible formation of PtOx.
Figure S3. Cross-sectional SEM analysis of a) layered-composite and b) co-sprayed composite of 30 wt% Pt-CNT-CsH2PO4 from Strategies 1 and 2, respectively, illustrated in Scheme 2 in the main text. The straw-like layer is the carbon paper electrode and the thin white layer is the CsH2PO4-based electrode.
Figure S4. Symmetric cell impedance measurements of electrosprayed commercial CNTs (as received). Measurements are performed at 240 °C in a dynamic atmosphere of 0.4 atm H2O and balance H2 supplied at a gas velocity of 6 cm min-1 (inset: equivalent circuit used for fitting).
1. A. Varga, N. A. Brunelli, M. W. Louie, K. P. Giapis and S. M. Haile, J. Mater. Chem., 2010, 20, 6309.
