Supplementary Material (ESI) for CrystEngComm This journal is © The Royal Society of Chemistry 2010
Supporting document for Large-Scale Synthesis of Feather-like Single-Crystal Te via a Biphasic Interfacial Reaction Route Shun Wang a∗ Kejun Zhang a Huan Zhou a Weipeng Guan a Dekun Ma a∗ Juanjuan Lin a Lijie Zhang a Shaoming Huang a and Jichang Wang b* a
Nano-materials & Chemistry Key Laboratory, Wenzhou University, Wenzhou, Zhejiang, China 325035; Department of Chemistry and Biochemistry, University of Windsor, ON, Canada N9B 3P4
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Figure S1. The XRD pattern of the as-prepared product. The reaction time was 3 hours and the reaction temperature was 120 °C.
∗
corresponding authors:
[email protected], fax: 86-577-88373064.
[email protected], fax 85-577-88373111.
[email protected], fax 1-519-973-7098.
Supplementary Material (ESI) for CrystEngComm This journal is © The Royal Society of Chemistry 2010
Figure S2. EDS analysis of the feather-like Te products.
Figure S3. SEM micrographs of the Te products prepared via reducing TDEC with different reducing agents: (a, b) thiophenol, and (c, d) phenylsulfinic acid. The reaction temperature was 120 °C and the reaction time was 16 hrs.
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Supplementary Material (ESI) for CrystEngComm This journal is © The Royal Society of Chemistry 2010
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2θ (degree) Figure S4. XRD pattern of the Te products prepared via reducing TDEC with different
reducing agents: (a) thiophenol, and (b) phenylsulfinic acid. The reaction temperature was 120 °C and the reaction time was 16 hrs.
Figure S5. SEM images of the Te products prepared under different pH values: (a) 11 and (b) 12. The reaction time was 3 hours and the temperature was 120 °C.
