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No Fe2Al5-xZnx inhibition layer formation was observed. During hot dip galvanizing in Zn-0.20%Al, the c-xMnO.SiO2 (x>1) oxide film was also reduced and the.
CORROSION SCIENCE AND TECHNOLOGY, Vol.11, No.1(2012), pp.1~8
Development of Continuous Galvanization-compatible Martensitic Steel Y. F. Gong1, T. J. Song1, Han S. Kim1, J. H. Kwak2, and B. C. De Cooman1,† 1
Materials Design Laboratory, Graduate Institute of Ferrous Technology, Pohang University of Science and Technology, Pohang, South Korea 2 Automotive Steel Research Group, POSCO Gwangyang Works, Gwangyang, South Korea (Received August 3, 2009; No Revision; Accepted February 24, 2012) The development of martensitic grades which can be processed in continuous galvanizing lines requires the reduction of the oxides formed on the steel during the hot dip process. This reduction mechanism was investigated in detail by means of High Resolution Transmission Electron Microscopy (HR-TEM) of cross-sectional samples. Annealing of a martensitic steel in a 10% H2 + N2 atmosphere with the dew point of -35 ℃ resulted in the formation of a thin c-xMnO.SiO2 (x>1) oxide film and amorphous a-xMnO.SiO2 oxide particles on the surface. During the hot dip galvanizing in Zn-0.13%Al, the thin c-xMnO.SiO2 (x>1) oxide film was reduced by the Al. The a-xMnO.SiO2 (x1) oxide film was also reduced and the amorphous a-xMnO.SiO2 and a-SiO2 particles were embedded in the Fe2Al5-xZnx inhibition layer formed at the steel/coating interface during hot dipping. The results clearly show that Al in the liquid Zn bath can reduce the crystalline c-xMn.SiO2 (x>1) oxides but not the amorphous a-xMnO.SiO2 (x
