Determination of Effective Thermal Conductivity of

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Chair of Engineering Thermodynamics. Institute of Thermal Engineering. Determination of Effective Thermal. Conductivity of Open-Cell Foam Ceramics. P. Götze ...
Chair of Engineering Thermodynamics Institute of Thermal Engineering

Determination of Effective Thermal Conductivity of Open-Cell Foam Ceramics P. Götze, V. Skibina, R. Wulf, M. Emmel, U. Gross, C.G. Aneziris TU Bergakademie Freiberg 20-23. Mai 2012

International Symposium on Ceramic Materials and Components for Energy and Environmental Applications

Table of Contents

Transient-Plane-Source Technique (TPS) Preliminary Measurements Preparatory Activities TPS Measurements Summary

SFB920 Multifunctional Filters

P.Götze λeff of Open-Cell Ceramics

TTD/IWTT TU Bergakademie Freiberg

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Investigated Materials Preliminary Measurements

Carbon-bonded Al2 O3

Phosphate-bonded Al2 O3

Both: > 87, 9% open porosity 10 and 30 PPI SFB920 Multifunctional Filters

P.Götze λeff of Open-Cell Ceramics

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Measurements of Phosphate-Bounded Al2 O3 Preliminary Measurements 0.6 eff

ungrinded AOF 10ppi AOF 30ppi

in W/(m K)

0.5

0.4

0.3

0.2

0.1

Øsensor in mm

0.0 0 SFB920 Multifunctional Filters

10

20 λeff

30

P.Götze of Open-Cell Ceramics

40

50

60

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Measurements of Phosphate-Bounded Al2 O3 Preliminary Measurements 0.6 ungrinded AOF 10ppi AOF 30ppi

cp in MJ/(m³K) 0.5

0.4

0.3

0.2

0.1 Øsensor in mm 0.0 0 SFB920 Multifunctional Filters

10

20 λeff

30

P.Götze of Open-Cell Ceramics

40

50

60

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Detection of Optimal Sensor Size TPS Measurements 0.7 eff

in W/(m K)

0.6

ungrinded

grinded

AOF 10ppi

AOF 10ppi

AOF 30ppi

AOF 30ppi

0.5

0.4

0.3

0.2

0.1

0.0 0 SFB920 Multifunctional Filters

10

20

30

P.Götze λeff of Open-Cell Ceramics

40

50

Øsensor in mm 60 70

TTD/IWTT TU Bergakademie Freiberg

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Detection of Optimal Sensor Size TPS Measurements 0.7 cp in MJ/(m³K)

ungrinded

grinded

0.6

AOF 10ppi

AOF 10ppi

AOF 30ppi

AOF 30ppi

0.5

0.4

0.3

0.2

0.1 Øsensor in mm

0.0 0 SFB920 Multifunctional Filters

10

20 λeff

30

P.Götze of Open-Cell Ceramics

40

50

60

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10

Effective Thermal Conductivity over PPI TPS Measurements 0.7 eff

Grinded Material

in W/(m K)

øSensor= 12,806 mm øSensor= 29,220 mm

0.6

0.5 AOF 0.4

0.3 LDF 0.2

AOF

0.1

LDF

0.0 5 SFB920 Multifunctional Filters

10

15 λeff

20

P.Götze of Open-Cell Ceramics

25

30

TTD/IWTT TU Bergakademie Freiberg

PPI

35

11

Summary

Preliminary Measurements Specimen–sensor coupling important Effective thermal conductivity λeff λeff,AOF > λeff,LDF λeff increases with PPI number Outlook Enhance contact specimens–sensor Determine optimal measurement parameters Conduct high temperature measurement

SFB920 Multifunctional Filters

P.Götze λeff of Open-Cell Ceramics

TTD/IWTT TU Bergakademie Freiberg

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Acknowledgment

The author would like to thank the German Research Foundation (DFG) for supporting these investigations (CRC 920, Subproject B03). Furthermore, thanks also go out to: A. Hegewaldt1 , F. Luthardt2 , G.Standke2 , M. Gröpper1 , S. Kielau1 , N. Bräutigam1 1 2

TU Bergakademie Freiberg Fraunhofer IKTS

Download presentation: http://tu-freiberg.de/fakult4/iwtt/ttd/ Further information CRC 920: http://tu-freiberg.de/ze/sfb920/index.en.html

SFB920 Multifunctional Filters

P.Götze λeff of Open-Cell Ceramics

TTD/IWTT TU Bergakademie Freiberg

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Detection of Optimal Sensor Size TPS Measurements 60.0 a in mm²/s 50.0

ungrinded

grinded

AOF 10ppi

AOF 10ppi

AOF 30ppi

AOF 30ppi

40.0

30.0

20.0

10.0 Øsensor in mm 0.0 0 SFB920 Multifunctional Filters

10

20 λeff

30

P.Götze of Open-Cell Ceramics

40

50

60

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Detection of Optimal Sensor Size TPS Measurements 0.5 eff

in W/(m K)

ungrinded LDF 10ppi LDF 30ppi

0.4

grinded LDF 10ppi LDF 30ppi

0.4 0.3 0.3 0.2 0.2 0.1 0.1 Øsensor in mm

0.0 0 SFB920 Multifunctional Filters

10

20 λeff

30

P.Götze of Open-Cell Ceramics

40

50

60

TTD/IWTT TU Bergakademie Freiberg

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17

Detection of Optimal Sensor Size TPS Measurements 0.50 cp in MJ/(m³K) 0.45

ungrinded LDF 10ppi LDF 30ppi

grinded LDF 10ppi LDF 30ppi

0.40 0.35 0.30

0.25 0.20 0.15 0.10 0.05 Øsensor in mm 0.00 0 SFB920 Multifunctional Filters

10

20 λeff

30

P.Götze of Open-Cell Ceramics

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50

60

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Detection of Optimal Sensor Size TPS Measurements 8.0 a in mm²/s

ungrinded LDF 10ppi LDF 30ppi

7.0

grinded LDF 10ppi LDF 30ppi

6.0 5.0

4.0 3.0 2.0 1.0

Øsensor in mm

0.0 0 SFB920 Multifunctional Filters

10

20 λeff

30

P.Götze of Open-Cell Ceramics

40

50

60

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Detection of Optimal Sensor Size TPS Measurements 0.7 eff

Grinded Material LDF 10ppi AOF 10ppi LDF 30ppi AOF 30ppi

in W/(m K)

0.6

0.5

0.4

0.3

0.2

LDF

AOF

0.1 Øsensor in mm

0.0 0 SFB920 Multifunctional Filters

10

20 λeff

30

P.Götze of Open-Cell Ceramics

40

50

60

TTD/IWTT TU Bergakademie Freiberg

70

20