Fragmentation & Pulverization

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(a) In the process of fragmentation, clusters split up into parts of a certain fraction. (b) The reverse dynamics, 'fractional percolation. In contrast to ordinary ...
Fragmentation & Pulverization

H O. Ghaffari With W.A.Griffith &Troy J. Barber

Dec 2016

Fragmentation :a wide range in nature

(a) In the process of fragmentation, clusters split up into parts of a certain fraction. (b) The reverse dynamics, ‘fractional percolation. In contrast to ordinary aggregation processes, in fractional percolation the coalescence of clusters that substantially differ in size is systematically suppressed.

“Pulverization of chromosomes in micronuclei may also be one explanation for ‘chromothripsis’ in cancer and developmental disorders, where isolated chromosomes or chromosome arms undergo massive local DNA breakage and rearrangement”.

Qin, Z., Pugno, N. M., & Buehler, M. J. (2014). Mechanics of fragmentation of crocodile skin and other thin films. Nature’s Scientific reports, 4.

Theories of Fragmentations

(Key-Schultz,2011)

Fragmentation :a wide range in nature

(PRL,2006)

Onset of Reflection of Incident Signal

Reflected signals in Incident bar

Fragmentation :a wide range in nature

(PRL,2006)

(epl,2008)

Fragmentation Topological Vortex Defects in Ferroelectric

Dependence of the defect density nv on cooling rate (Nature Physics ,2015) (PRL,2010-PNAS 2009)

(PRX,2014) -leveling off : saturated min.fragment’s size -suppression of defect formation : controlling fragmentation

Fragmentation :a wide range in nature

(PRL,2010-PNAS 2009)

Coloring the domains(fragments) : a new method to characterize the fragments

The famous four-color theorem states that all regions of every two-dimensional map can be colored with only four colors in a manner that no two adjacent regions have the same color (Apple-Haken theory,1976)

Heavily crumpled surfaces analogous with heavily fragmented solids

Ridge networks : fracture networks

Ridge networks formed in flattened crumpling sheets of size L=8 1, 16 2, and 35 3 cm of Albanene-1 paper. B

PHYSICAL REVIEW E 74, 061602 2006

crumpled surfaces are analogous to Spin field undulation Useful analogy of crumpling with Heisenberg ferromagnetism : the direction of growth or decay is the surface normals (i.e., spin field), and a crumpled surface is similar to a Heisenberg paramagnet. Therefore, destroying long-range order of surface normals are in analogy with spin waves.

Kantor, Y. and Nelson, D.R., 1987. Crumpling transition in polymerized membranes. Physical review letters, 58(26), p.2774.

fragmentation to pulverization Transition : coloring domains approach Transition to Fragmentation Transition to Pulverization

Finite domains Pulverized state == max. Fragmentation

Finite domains

I

I

2d system II (direct transition)

Heavily fragmented

Stress Pulse(Destructive)

III

III Partially /fragmented pulverized (mixed state)

Impulsive loading ?

Stress (i.e., Creep/plastic deformation)

1d system:

 Phase diagram of Solid-Granules Transition (s-g transition) U

 Fragmented regime is broken symmetry

M

 initial state: is symmetric state

I

U

Finite domains

I

M

II (direct transition)  Pulverized state: is another ordered state Stress Pulse(Destructive)

III

III Partially pulverized or fragmented/mixed state

 Pulverized state ==

max. Fragmentation = Anti-ferromagnetic state 2d system

1d system:

Imaginary state in s-g transition ...  ...  ...  ... ...  ...  ...  ...

Ordered sate

U

Finite domains

M

 initial state: is symmetric state

I

U

I real situation in s-g transition

M

II (direct transition)

 Pulverized state: is another ordered state

Stress Pulse(Destructive)

III

III Partially pulverized or fragmented/mixed state

 Phase diagram of Solid-Granules Transition  Possible existence of Tipple point in fragmentation-pulverization transition

J 0

J 0

J 0

II

Energy

U

I J 0

M

U

I

J 0

M

  Minimum size of a fragment is a unit cell in lattice structure

 Another possibility of Phase diagram of Solid-Granules Transition :modulated state and shape of domains modulated state

..  ..

modulated state II

Energy

..  .. U

I M

U

I M

 U

M

modulated state U

M

 Fragmentation mediated granular flow : example soft rocks such as sandstone

Crystalline Solid

Fragmented Solid Critical point I

Floating solid

Critical point II

 Frozen impurities in these types of Models : Spin glasses

Stress (or impulse rate)

Fragmentation to Pulverization : Solid-granules transition

(Aben et al,2016)

Evolution of strain energy along the loading path (dashed line) and its changes under small strain perturbations around points with markers (out of scale). The flattening of the parabolas around markers 3 and 4 represents material degradation due to damage increase compared with undamaged material (markers 1 and 2). (Lyakhovsky,1 Yehuda Ben-Zion,2016).

 Fracture mechanics aspects of Solid-Granules Transition



 Rice 1975; Bhat etal.2012

 Gd    (2  surface 

G  2 surface  wInelastic



G  K I2 “Toughening” term (s) due to inelastic regime in a main/major crack tip due to micro-cracks ;



Perfect-Elastic Inducing domains during pressure-quench (P-impulse)



G  2 surface G  K I2



0

surface

 wInelastic )d 

 Fracture mechanics aspects of Solid-Granules Transition  initial state: is symmetric state

R=1

 The maximum number of fragmentation is obtained by the pattern of (d) which is in analogy with pulverization. In terms of spin models, the ideal pulverization resembles antiferromagnetic: an ordered state.

Anti- ferromagnet : Ising model with metropolis algorithm

Fragmentation in 1D system

Background noise Control Parameter

Rise time of the pulse

VGinzburg  Landau ( )      2

4

Formation of kinks in a 1-D Landau-Ginzburg system VGinzburg  Landau ( )      2

4

 driven by white noise.

with real

Overdamped Gross-Pitaevskii evolution with

  t /  Q and:

  c      2    noise 2

2

2

(Laguna-Zurek, 1997)

very fast stress loadings are ‘‘all impulse,’’ and—according to Dynamic transition model —the number of kinks should saturate.

(Laguna-Zurek, 1997)

G-L framework and its connection with Phase field model

 t k ( xi , t )   2 ki  

 2

g (ki )( i 2   c2 ); g (ki )

 ui ui   b    .[ g ( k )  (1   t )ui ] i t 2 t  2

ki  ;  i  ui

Approach II: Define the characteristics of the “domains” with their phase using velocity vectors A thin-film

vi

strain-control ring

Rock Sample

Prior to fragmentation/ pulverization Onset of the impact of the fragments on the film ;



We assume similar size of the fragments but different velocity vectors

Exaggerated shape of the film in 2+1D

 The shape of the contour serves as the order function

ˆ

  

vibration modes of the “contour” v.s stress pulse

(

d )* dt

Colliding and Impact formulation Hertezian’s Contact

vi vi



Elastic Impact

R2   

1 1  R R1

Velocity of approach

Aluminum foil /pressure film as the thin sheet

Control Ring+ pressure thin film

A thin-film Longitudinal strain-control ring Rock Sample

i

Control Ring+ pressure thin film

b)

d) WG-6

WG-5

WG-2

WG-4

WG-1

Increasing ramp-rate

Ghaffari-Griffith-Baraber , in revision

Damage parameter from Patterns o pressure films

dD(t ) dl  D(t ) 2 / 3 D1/0 3 dt dt Rate of Growth of domain walls

Bulk damage

D(t )  1 

 A (t ) w

Atotal

 (t )   t

dD( ) dl  D( ) 2 / 3 D1/0 3 d d

Slope of D-e proportional to growth of domains

Damage parameter from Patterns o pressure films

 

  D(t )  0 L

D(t ) 

3   0.43 L 7 

 (t )  1

 (t )  1  Therefore,

1

 A (t ) w

Atotal

D

D(t ) 

  1 L

 (t )  1

Damage Parameter

Order Parameter

BET (surface area ) vs. patterns of thin films

Why sort of correlation?

 fractional BET on Prescaled film

a)

b)

c)

vn   n

vi

   vs   s

 max

 max



 max

  max  Sconatct

Imprinted surface area



S real  4 ( ) 2 2 BETreal

 Approximated contact surface area



2 r... r 2

4 ( ) 1 1 2    4   r  (  )3 3 2 2 2

 n ....

n 2

BETmapped 

r r

 (vapp. ) 2

(

3  ( ) )  4 r 2 r2

 2

 max  (

15mV 2 app

16   

1/ 2

E

*

)2 / 5 ,

 Patterns of film hold both information of formed fracture surfaces and kinetic energy

Inferring Normal and Tangential colliding velocity of exerted fragments : Estimating Kinetic Energy term

15mV 2 app

 max  ( )2 / 5 , 1/ 2 * 16    E P(r ,  ) 

3 2

4 K (r , ) 2 (r , )  (   1)    2   2

 With assuming a max. allowed indentation depth and having calibrated pressure films ,we can estimate an interval of colliding normal velocity

Approximation of fragment distribution

Measured Distribution

Estimated Distribution

Ghaffari-Griffith-Baraber , in revision

Inferring Normal and Tangential colliding velocity of exerted fragments : vn   n    vs   s

 In current calculation vs  0  But any shear component on an exerted particle adds a second terms to kinetic energy .  If the heat energy is due to frictional forces between fragments ,then we can assume a shear (rotational) component is added to net force (and then velocity vector ) which results an oblique impact of particles. The corresponding shear penetration  s might be estimated using estimated frictional heat:

s

NW f 

n

 Here the bar sign is average over all over fragments and N is the number of fragments.  In current calculation:

 MC simulation using a well defined distribution over fragments with having mean value of Vs from dissipated energy and BET analysis

Ek 

1 N 1 N 2 2 m ( v  v )  mi vn2  i n s 2 2 i 1 i 1

 i  ei  

A “phase”, therefore, can be extracted for each fragment

i

Spectrum of energy for fragmented and pulverized states (many-events spectrum) .  gaped states are eliminated in an ideal pulverized state.

Ghaffari-Griffith-Baraber , in revision

 Phase-transition from Intact state (I-state) to the pure pulverized state (P-state).  Here, we assumed the system moves on a rigid energy landscape. In reality, the energy landscape is not rigid.