Single Cotton Fiber Properties of Low, Ideal, and High Micronaire Values JONNA. FOULK'
AND
DAVIDD. MCALISTER ID
USDA, ARS, Cotton Quality Research Station, Clemson, South Carolina 29633, U.S.A. ABSTRACT The Favimat, a single fiber testing machine, is used to quantify the affects of cotton crimp on fibers from three samples consisting of cottons containing low, high, and ideal micronaire values for textile processing. In order to get a better representation of all fibers within these samples, the cotton is further divided into the Suter-Webb array length groups. Following cotton crimp image capturing, fiber fineness is determined by the vibroscope method. The mean values for these samples indicate that cotton containing more crimp in the fibers leads to larger elongation, force to break, linear density, tenacity, and work to rupture. The seven length groups from these cottons indicate that longer cotton fibers appear to contain more crimps per cm. The results suggest that the Favimat is satisfactory for measuring current and future cotton properties.
Once-over cotton harvesting removes all cotton bolls from the plant [25], with mature cotton bolls found near the base and stem of the plant and natural variations of immature cotton bolls throughout the plant 1381. Cottonseed hairs (fibers) are removed, separated, and cleaned from cotton bolls by ginning to form cotton bales containing fibers from the entire plant. Cotton bales used in textile processing may contain diverse cotton fiber varieties grown on differing soils under different environmental conditions with varying fertilizer application rates and harvesting at different rates. Textile processing requires these diverse cotton bales to be blended, cleaned and processed, aligned, drawn, and twisted to form uniform yarns. Yarn strength is determined by fiber strength and fiber interactions, including length, friction, and twist [19]. Attempts have been made to correlate yarn strength and single fibers [35]. Yarns typically use approximately 30 to 70% of single fiber strength [19]. With increased processing speeds, cotton fiber classification improvements are required. Cotton grading has progressed from subjective human classers to the HVI, a high volume instrument. Prior to WI, classical cotton fiber properties such as strength, elongation, and fineness were generated by the Pressly tester, Stelometer, and Fibronaire. The WI and Stelometer physically test specially combed fiber bundles. Fibronaire and HVI measurements of fineness use known weights of cotton fibers. The Favimat (Textechno Herbert Stein GmbH & Co. KG, Monchengladbach, Germany), a low volume single fiber testing instrument,
provides single fiber values, which are not currently generated in cotton grading that tests fiber bundles. Prior to the Favimat, Textechno in Germany has produced single fiber testers since 1955 [27]. Dedicated single fiber testing instruments have progressed from the Dewey tester [16] to today's instruments, the Favimat and Mantism (Zellweger-Uster, Charlotte, NC). The Favimat provides traditional single fiber data, tensile strength, and percent elongation at a constant rate of extension with additional fiber parameters such as capturing fiber crimps, tenacity, linear density, and work to rupture in approximately 35 seconds [41]. It was developed and is currently used for testing the consistency of synthetic fiber production [27] with its potential use in cotton testing unknown. Fibers may be manually or mechanically loaded [9] into the Favimat. The machine has the ability to test and differentiate single fibers based on tensile strength, fineness, crimp extension, crimp rigidity, and crimp number on the same fiber section [ l l , 36, 391. Many events impact cotton fibers, so a better understanding of the consequences is needed to expedite processing in textile mills and to encourage certain cotton varieties. Reversals and convolutions are interrelated, so a cotton convolution occurs when many cellulose layer reversals overlap [19]. Upon drying, the convolution angle of cotton fibers increases, which decreases the force to break these fibers [12]. Shenai [37] declared that cotton spins better with more convolutions and Afzai [I] believed cotton breeders should try to develop new con' Corresponding author: tel.: + 1-864-656-2488, fax: + 1-864-656- voluted varieties. A fusion of convolutions and reversals 1311, e-mail:
[email protected]. results in cotton crimp.
Textile Res. J. 72(10), 885-891 (2002)
Cotton hairs grow to various lengths from cells on the 221. Dehydration of the spiral wall structure creates a seed to form elongated tubular shapes that appear as distorted cross-sectional area, which causes the fiber to solid rods (circular cross section). These fibers are not twist about its axis, forming a twisted and convoluted solid, but hollow, and twist and crimp when dried. Often ribbon [33, 43, 22, 191. All fibers lose their circular overlooked, fiber crimp, waviness, or kinkiness is a cross-sectional shape when dried, but immature fibers known fiber parameter that affects fiber cohesion [29]. generate pronounced cross-sectional differences from Crimp is characteristic of all cotton fibers and determines mature fibers [22]. Coarse cotton fibers typically have the capacity of fibers to adhere under light pressure. The fewer convolutions than fine fibers, with fiber friction consistency and coherence of card webs, sliver, and increasing with convolutions [20]. Basu et al. [lo] demroving and the strength and hairiness of yarn are all onstrated that the frictional characteristics of cotton fiaffected by a fiber's crimp. Crimp has been measured as bers depend on the occurrence of convolutions. number of crimpslcm or as a percent increase in the The uneven exterior of a dry cotton fiber's structure extent of the fiber up on crimp removal [ l l , 291. The contains parallel wrinkles at a slight angle to its axis [43]. number and frequency of convolutions and reversals may The formed helical structure directly relates to fiber be a function of the environment [26]. Growth conditions reversals, random inversions of fiber wrinkles as deendured by cotton plants may influence the crimp found scribed by Waterkeyn [43], and convolutions, twists of a in cotton hairs. fiber through 180" about its axis as described by Cotton fiber development commences and develops in Meredith [24]. These reversals are related to the oriena known order. Following flowering, each individual cell tation of secondary walls [19] and represent zones of expands longitudinally for 25-35 days [23]. The ultimate variation in breaking strength [22, 191. Regions adjacent length is determined by the cotton variety and environ- to these reversals are constricted, of a lower density, and mental conditions. During this growth, the cells are en- the weak point of the fiber rather than the reversal itself circled by a primary cell wall and covered by a waxy [19]. Increases in cotton convoIutions have been linked layer or cuticle [22]. A secondary wall begins inside the to increased fiber strength [14, 191. primary wall as each fiber reaches its maximum length, The objective of this study is to evaluate testing prosolidifying for 30-50 days [23]. Cellulose in the crys- cedures and results generated by the Favimat, a new talline state begins to form 15-19 days postanthesis, and single fiber instrument. Cotton samples of three different by maturity, tubular fibers contain 96% cellulose [22] micronaire values are selected to cover a range of cotton with 90% in the secondary wall [21]. fineness and to determine if different micronaire values Immature fibers have thin secondary walls, while ma- influence single fiber results. Favimat analysis of crimp ture fibers have secondary walls approaching maximum is advantageous for synthetic crimped fibers, and this thickness [29, 221. Shorter cotton fibers are often con- study explores the generation of cotton results. sidered weak and immature with a less circular cross section and low linear density [32]. Fibers of a higher Materials and Methods maturity level demonstrate higher strength and linear density than immature fibers [19]. Cellulose molecules Three commercial southeastern cottons used in this run parallel along the axis of the fiber [17]. Lewin and study consisted of upland varieties from the 1998 and Pearce [22] stated that the secondary wall, which forms 1999 harvest. These cottons differed in fineness as meathe main body of the fiber, consists of nearly parallel sured by the micronaire method, and were all harvested, fibrils laid down concentrically in a spiral formation. ginned, and baled by commercial methods (see Table I Two layers are deposited daily in opposite directions, for official USDA AMS HVI data). These three samples were with a dense layer deposited at night and a less dense chosen for their micronaire diversity because each cotton layer during the day [37]. Cellulose molecules make up represented a low (3.7), ideal (4.3), or high (5.4) micronthe cell walls, forming crystalline microfibrils that are aire for textile processing. For ease of classification, arranged in a complex multilayer structure [17, 221. these cottons are referred to as I, 11, or 111, respectively. Strength and elongation increases with the increasing Prior to testing, all cotton samples were conditioned for crystalline microfibril spiral arrangement and orientation at least 48 hours at 65% RH and 21°C 161. within the cotton fibers [37]. Picking a single fiber from cotton samples often reMature cotton bolls dehisce, which exposes the fibers sults in selecting the mature, long, strong fibers that are to prevailing environmental conditions [22]. Upon de- often the easiest to separate. In order to get a better hiscing, seed fibers lose their moisture, causing them to representation of all fibers within these samples, the collapse, curl, and wrinkle, producing folds, convolu- cotton was further divided into the Suter-Webb array tions (twists), and compression marks in the fibers [33, length groups [7]. A Fibroliner FLlOl (Peyer Electron-
887 TABLEI. Official USDA AMS cotton classification dataa cottonb
Crop year
Mic
Strength
Color
Color quadrant
Rd
+b
Trash
UHM
UF
Leaf
1998 1998 1999
3.7 4.3 5.4
26.0 25.7 27.6
41 32 42
3 2 2
73.5 74.3 72.5
89.0 95.0 88.8
7 5 3
99.0 103.0 104.5
79.0 80.0 80.5
5 3 3
--
I I1 111 a
USDA, AMS, Memphis, TN.
Cottons of low (3.7). ideal (4.3), and high (5.4) micronaire are referred to as I, 11, or 111, respectively.
ics, Spartanburg, SC) was used to help separate the fibers [8]. For fiber alignment, a 90 mg sample was inserted into the Fibroliner to be combed and sorted twice. Following alignment, this fiber beard was pulled twice, removing the longest fibers. These fibers were removed from the combs and placed on a black velvet board to be measured with a Suter-Webb array ruler graduated in 0.3175 cm. Repeatedly, these pulls removed the longest fibers remaining in the fiber tuft, allowing fiber separation and storage into Suter-Webb array length groups 7, 9, 11, 13, 15, 17, and 19. All fibers shorter than 0.9525 cm were placed in length group 7. The Favimat measures the amount of force required to break up to 210 cN with a resolution of 1 X 10-4, while the fineness of these same fibers can be measured from 0.5 to 200 dtex. In a manner similar to the Mantis, tensile strength is determined using a constant rate of extension. A gauge length of 10 mm and cross-head speed of 20 mmlmin under a pre-tension of 0.20 cNItex were used in testing. Fiber fineness was determined by the vibroscope method [5]. Crimp number and amplitude were determined with an opto-electrical sensor that evaluates the fibers under 0.03 cN1tex. Twenty-five fibers from each cotton and each different length group were tested twice using the Favimat standard tensile test procedure [40]. After loading, the testing period was approximately 35 seconds per fiber. For Favimat single fiber testing and ease of separation, a small tuft of fibers from one length group was laid on a black velvet board. Using forceps, a single fiber was randomly separated from the group of fibers, and a small clip weighing 50 mg was attached to the far end of the fiber. Forceps were used to grasp the opposite end of the fiber for Favimat mounting. The 50 mg clip kept the fiber straightened under constant tension for securing into the Favimat. The upper Favimat clamp was closed, which suspended the fiber and clip. Both upper and lower clamps had a clamping surface area of 16 mm2 with soft and hard rubber faces. Closing the bottom Favimat clamp initiated Favimat single fiber testing. The data were statistically analyzed with the general linear models procedure in SAS using Duncan's new multiple range test (P < 0.05) to detect differences between means [34].
Results Single fiber Favimat procedures were tedious but did produce comparable fineness, elongation, and tenacity results in a relatively short period. Manually separating the fibers into their length groups, preparing the fibers for testing, and loading the fibers into the Favimat were the most difficult and time-consuming processes. Future studies with the new robotic portion of the Favimat would help streamline the process. Once a fiber was loaded, no intervention occurred, with all testing performed sequentially on the same fiber section. The Favimat is self-contained to test fiber fineness, tenacity, force to break, work to rupture, and crimp as a reasonable method for gathering single cotton fiber data. Modifications to current testing parameters present the potential for additional research, as do further single fiber Favimat tests such as crimp stability and crimp extension. In each cotton, fifty fibers from the seven length groups provided approximately 350 single fiber properties for each of the three cottons (Table 11). With this sample size, length groups only begin to form a trend. In order to better visualize this trend, Suter-Webb array length groups 7, 9, 11, 13, 15, 17, and 19 were all averaged across length groups and combined into their three respective cotton categories to evaluate single cotton fiber differences. Assessed Favimat fiber quality parameters for the three diverse micronaire cottons tested in this study are listed in Table 111. In order to better compare these single fiber results to bulk fiber bundle tests, the number frequency distributions must be determined across length groups. Measuring single cotton fibers on the Favimat showed that the force to break the cotton significantly increased from cottons I through 111. Cotton I had the lowest mean force to break of 3.86 g, followed by cottons I1 and 111 with respective mean force to break values of 4.34 and 5.20 g. Cotton I elongated the least, 7.42%, followed by cotton 11, 9.04%, and cotton 111, 9.51%. Single fiber elongation values from cottons I1 and I11 were significantly different from cotton I. Subsequently, in evaluating work to rupture, samples from cottons I, 11, and I11 were statistically different, increasing from cotton I (0.16 gYcm)to cotton I1 (0.22 gYcm)to cotton 111 (0.27 gYcm).
TEXTILE&SEARCH JOURNAL TABLE11. Effect of Suter-Webb length group cotton fibers via Favirnat. Cottona I
Length groupb
Sample number
Force to break,' g
Elongation,' %
Linear density,' dtex
Crimp: crimplcm
7 9 11 13 15 17 7 9 11 13 15 17 19 7 9 11 13 15 17 19
50 50 50 50 50 50 49 50 50 49 50 50 48 49 48 50 50 48 48 50
3.98 e,f,g 3.92 e,f,g 4.01 e,f,g 3.69 g 3.71 g 3.85 f,g 4.28 d,e,f,g 4.75 b,c,d,e,f,g 4.35 c,d,e,f,g 4.37 c,d,e,f,g 4.05 e,f,g 4.46 c,d,e,f,g 4.15 d,e,f,g 5.35 a,b,c 5.13 b,c,d 6.10 a 4.29 d,e,f,g 4.97 b,c,d,e 5.69 a,b 4.89 b,c,d,e,f
7.05 g 7.34 f,g 8.03 d,e,f,g 7.24 f,g 7.38 f,g 7.5 e,f,g 9.05 b,c,d 9.18 a,b,c,d 8.82 c,d,e 9.1 1 b,c,d 9.01 b,c,d 9.14 b,c,d 8.97 b,c,d 9.32 a,b,c,d 8.53 c,d,e 10.60 a 8.87 c,d,e 9.89 a,b,c 10.48 a,b 8.87 c,d,e
1.70 c 1.71 c 1.73 c 1.66 c 1.54 c 1.58 c 2.28 a,b 2.15 a,b 2.06 b 2.28 a,b 2.1 1 a,b 2.31 a,b 2.17 a,b 2.16 a,b 2.36 a 2.31 a,b 2.28 a,b 2.36 a 2.19 a,b 2.1 1 a,b
11.23 e,f 11.66 c,d,e,f 10.95 f 11.29 d,e,f 11.51 c,d,e,f 11.63 c,d,e,f 11.71 c,d,e,f 12.15 b,c,d,e 12.83 a b 12.22 ab,c,d,e 12.62 ab,c 12.40 ab,c,d 12.43 ab,c 12.37 ab,c,d 12.60 ab,c 12.62 ab,c 12.40 ab,c,d 13.02 a b 13.02 a b 13.32 a
Seven length groups correspond "Cottons of low (3.7), ideal (4.3), and high (5.4) rnicronaire are referred to as I, 11, or 111, respectively. to Suter-Webb length groups [8]. "Values followed by different letters within columns are significantly different, P < 0.05, according to Duncan's new multiple range test.
TABLEIII. Effect of different rnicronaire cottons on single cotton fiber properties via Favirnat. Cottona
Sample number
Force to break,b gforce
~lon~ation,b %
Linear d e n ~ i t y , ~ dtex
Tenacity: gforceltex
a Cottons of low (3.7), ideal (4.3), and high (5.4) rnicronaire are referred to as I, II, or III, respectively. within columns are significantly different, P < 0.05, according to Duncan's new multiple range test.
Fiber fineness measured by the vibroscope method indicated linear density increased from 1.66 dtex in cotton I to 2.19 dtex in cotton I1 and 2.25 dtex in cotton 111. While these linear density values were unlike traditional airflow principals, they confirmed the same fiber fineness progression. Results indicate that force to break, fineness, and elongation of single fibers are closely related. In order to better compare linear density values to traditional airflow fineness values, the frequency distributions must be determined across length groups. Convolutions and reversals in cotton fibers create fiber crimp that statistically increases from cotton I (11.38 crirnplcm) to cotton I1 (12.34 crimplcm) and cotton I11 (12.76 crimplcm). The cottons influence the measured Favimat parameters with statistical differences existing between the three diverse rnicronaire cottons. Single fiber properties appear to be a function of the cotton tested and possibly of crimp. Crimp is known to affect friction and thus drafting and yarn processing. Yarns are influenced by frictional properties and less hairy if highly
Work to rupture? gcrn
Crimp? crimp/cm
Values followed by different letters
crimped fibers are used. The mean values for these three samples indicate that cotton containing more crimp in the fibers leads to larger elongation, force to break, linear density, tenacity, and work to rupture. Cottons I, 11, and I11 were all combined into seven respective length groups (7, 9, 11, 13, 15, 17, 19) to evaluate testing results. The outcome of these groups on Favimat single fiber analysis is shown in Table IV. After combining all cottons and separating them based on their length groups, there were no statistical differences in linear density and elongation values. Among force to break values, length group 11, 4.82 g, was the strongest and statistically different from the weakest length group 13, 4.12 g. Evaluation of single fiber tenacity illustrated that length group 7 had the highest tenacity of 24.57 gforceltex and was significantly different from length group 13 with 20.72 gforceltex. Length group 11 had the largest work to rupture of 0.242 g*cm which was significantly different from the length group 13 value of 0.196 g * cm.
OCTOBER 2002
889 TABLEIV. Effect of Suter-Webb length group cottons on single cotton fiber properties via Favimat.
Length groupa
Sample number
7 9 11 13 15 17 19
148 148 150 149 150 148 98
Force to break: g 4.53 a,b 4.59 a,b 4.82 a 4.12 b 4.24 a,b 4.65 a,b 4.53 a.b
Elongation: %
Linear density: dtex
8.46 a 8.35 a 9.15 a 8.40 a 8.76 a 9.02 a 8.92 a
a Seven length groups correspond to Suter-Webb length groups [8]. different, P < 0.05, according to Duncan's new multiple range test.
Measurements of crimp properties showed that length group 19 with 12.89 crimplcm was the largest and was significantly different from length groups 7 (1 1.77 crimp1 cm), 9 and 11 (12.13 crimplcm), and 13 (11.97 crimp1 cm). The mean values for these seven length groups indicate that cotton containing more crimp in the fibers may be related to longer fibers. Favimat single fiber properties combined together into short (fibers 1.60 cm and less) or long fiber categories (those fibers greater than 1.60 cm) demonstrate no statistical differences. Fibers 1.6 cm and less have a force to break of 4.65 g, a crimp of 8.66 crimplcm, and a linear density of 2.05 dtex. Longer fibers have a force to break of 4.37 g, a crimp of 8.76 crimplcm, and a linear density of 2.05 dtex. The lack of a trend or variation among length groups confirms that to provide the greatest benefit, additional work is necessary with other cotton samples in order to detemine if crimp influences fiber properties.
Discussion Cotton failure has been mainly studied as fiber bundles in cotton classification. Single cotton fibers have many potential weak points in their structure, conceivably related to growing conditions and variety. Cotton exhibits different cellulose packing densities with lower convolutions, reversals, and crimps within coarse varieties [311. Cotton fiber strength differences are due to crystalline structure and convolution differences among varieties [13]. Traditional fiber properties as well as crimp and linear density determinations on the same single fiber offer the potential for better fiber and yarn comprehension. Yarn evenness and strength are known to increase with fiber cohesion and may be a function of fiber crimp. As yarn frictional properties are better understood, this progression may initiate breeders to introduce other new cotton varieties. In our study of three cottons, it appears that samples containing more crimp in the fibers lead to larger elongation, force to break, linear density, tenacity, and work to rupture. This agrees with work by Cho et al.
Tenacity: gforceltex
Work to r ~ p t u r e , ~ g*cm
Crimp," crimplcm
2.04 a 2.07 a 2.03 a 2.07 a 2.01 a 2.03 a 2.14 a
Values followed by different letters within columns are significantly
[I41 and Hsieh [19], who have shown that increased cotton convolutions lead to increases in fiber strength. We prepared a single fiber for the Favimat with the entire fiber section tested under the same load. Morton and Hearle [28] have shown that finer cottons have a higher tenacity with elongation not related to fineness, while Favimat results indicate that fibers with more crimps may have higher linear density, tenacity, and elongation. Highly crimped fibers contain many convolutions and reversals that must undergo untwisting and extension during a test [31]. Fibers with higher crimp appear to have higher strength, which may clarify why Shenai [37] believes that highly convoluted cotton spins better. Favimat results agree with tenacity and linear density correlation work performed by Pate1 and Patil [30]. Single fiber tests performed on the Mantis and Instron have shown that as cotton fibers mature, the breaking force, elongation, work to rupture, linear density, number of twists, and convolution angle increase [19]. Fiber friction increases with convolutions, so crimp appears important to understanding yarn breaks because most fibers slip and a few fibers break. It is generally understood that commercial cottons contain the minimum crimp required for processing, with some cottons demonstrating an increase in convolutions with fiber length [15]. In our study, mean values for seven length groups indicate that cotton containing more crimp in the fibers may be related to longer mature fibers. Favimat measures the fineness directly on one fiber, while other fineness measurements are performed on a bundle of fibers. Single fiber Favimat tenacity properties all exceeded 6.12 gforceltex, the minimum tenacity required for fiber processing [19]. Morton and Hearle [28] implied that tenacity and elongation increase with longer cotton fibers, despite Favimat results indicating that these three cottons exhibit little or no tenacity or elongation increases with fiber length. Fiber property discrepancies between single and bundle fiber tests are likely to occur
due to cotton crimp. While differences in results exist, single and bundle fiber tests typically show a good correlation [42].
6.
Conclusions
7.
Crimp and other single fiber properties appear to be a function of the cotton tested. The mean values from these three diverse samples appear to suggest that a cotton containing more crimp in the fibers leads to larger elongation, force to break, linear density, tenacity, and work to rupture. As expected, results obtained on single fibers point to typical interrelationships of strength, length, and fineness. In addition, Favimat measurements of linear density and crimp count may prove helpful in predicting fiber strength for yarn processing. Future research requires numerous cotton varieties of diverse micronaire and length groups to determine cotton's ideal crimp and its association with synthetic fibers in textile processing. Crimped fibers require slightly less twist to form yarns and could help optimize production. Based on these testing procedures, the results suggest that the Favimat appears satisfactory for measuring current cotton properties. The results confirm the need for additional cotton variety, crimp analysis, and fiber microstructural research.
8.
9.
10. 11.
12.
13.
14. Mention of specific products is for information purposes only and is not to the exclusion of others that may be suitable. W e gratefully acknowledge Mark Reese and Mike Honeycutt from Lawson-Hemphill (Spartanburg, SC) for supplying the Favimat, Todd Westbrooks from Lawson-Hemphill for Favimat training and set-up, and Michael Baker of Voorhees College for technical assistance.
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