EDX computation explains

18 downloads 0 Views 76KB Size Report
Computation of apparent concentration K. ➢ K ratio : taking into account the standard composition and ZAF corrections on the standards dard s sample.
Example of quantification : TiNi alloy Interface of the SAMx /software IDFix Computation of apparent concentration K With Φ(ρz) model, the correction on a pure element is equal to 1 (thus Correction =1 for the standard)

Ki =

I sample I s tan dard

Intensities are in Counts/s/nA

.

=

.

K ratio : taking into account the standard composition and ZAF corrections on the standards

K ratio K iTi =

[email protected]

Ct [% w] = Ki × ZAFstd

1392,95 1,295 100% . . = 0,4352 2656,52 1,56 1

1

Example of quantification : TiNi alloy

2

Computation of the real concentration

For Titanium (Ti)

C [%w] = Z . A.F .sample ⋅ K ratio ⋅ ( x100)

0,9772 ⋅ ( x100) = 44,875% 0,9477

K = Kratio (pure elements are used as standards in Φ(ρz) model)

Abstract

=

C[%w] = 0, 4352 ×1 ×

.

. C[%w]=

Current and time corrections between standard and sample

[email protected]

.

%

(× 100) 2