FORMULATION DATA BASE CONTROL LIST

FORMULATION DATA BASE CONTROL LIST Formulation No TITLE 101 102 103A – K 104A - C 105 106 107A&B 108A&B, C, D 109 A - C 110 111A&B 112A&B 113A&B 114A&B 115 116 117 118 A & B 119 A & B 120 A & B 121 ABC 122 ABCD 123 AB 124 AB 125 AB 126 127 128 A&B 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148

.Low viscosity Furniture Polish Graffiti Remover Floor Polish Formulations Stainless steel cleaners Gel Hand Cleaner based on d-limonene Biocidal Hard Surface Cleaner Low Foam Rinse Aids, Domestic/Industrial dish washing Bottle Washing Floor Polish based on Lakewax 20 Engine Degreaser Shoe Polish Formulae Polish and Cleaner for Wooden Floors Low Foam Cleaner and wax srtripper Aluminium Cleaners (Alkali) Train Cleaner-Oxalic Non-Caustic Steam Cleaner Liquid Hand Soap Class Cleaners Laundry (Hotel & Restaurant) Cleaners Cream Cleansers Oven Cleaner Metal cleaner Immersion Metal cleaner Spray Metal Electrolytic Metal rinse aids Trailer Curtain Cleaner Low Foam Carpet Cleaners Laundry Detergents Machine dishwash Metal Working Heavy Duty Degreaser Insect Repellent Hard Surface Cleaner Anti-Graffiti Coating Polish for Wooden Floors Food/Dairy Cleaner Aluminium Degreaser De-scaler, Light Duty Wheel Cleaner Screen-Wash Formulation CAB, CTA/N-Personal Care Formulations Upholstery cleaner TFR CIP Steam cleaning, food , Dairy Abbatoir cleaners Low Foam Machine Parts Cleaner Low foam floor cleaner/wax stripper High Active Dishwashing Liquid Heavy Duty Laundry Detergent

149 150 151 A&B 152

Leather Care Treatments (Lakewax 20) Tile Cleaner Aluminium Cleaners Plastic Cleaner

101. Low Viscosity Furniture Polish Raw Material LAKEWAX 20 Water Emulsogen LP (1) White Spirit Silicone Oil Emulsion (E 1044, 35%) Antistatic Agent (Water soluble)

% Weight 30.0 17.0 2.5 30.0 20.0 0.5

The above milky white emulsion is suitable for filling into trigger and aerosol packs.

102. Graffiti Remover Raw Material LAKELAND AMA LF40 Water KOH (Flake) Dipropylene Glycol Monobutyl Ether Methanol Sodium Gluconate

Recommended dilutions:

% Weight 10.0 56.0 20.0 6.0 5.0 3.0

10 – 20 : 1

FLOOR POLISH Fmln No 103A HIGH SPEED FLOOR MAINTENANCE Excellent slip resistance and resistance to alcohol/water staining. Ingredients

Weight Percent

WATER

43.00

DIETHYLENE GLYCOL MONOETHYL ETHYL

4.40

TRIBUTOXYETHYL PHOSPHATE

1.10

1

FLUOROSURFACTANT (1% SOLUTION)

1.50

2

PROXEL GXL

0.10

1

MF 12 (38%)

42.00

LAKEWAX 37

7.90

TOTAL

100.00

Fmln No 103B DURABLE POLISH Low speed spray buffing or high speed maintenance. Ingredients

Weight Percent

WATER

36.97

DIETHYLENE GLYCOL MONOETHYL ETHER

6.50

TRIBUTOXYETHUL PHOSPHATE

1.90

FLUOROSURFACTANT (1% SOLUTION)

0.80

1

PROXEL GXL

0.10

2

TEGO FOAMEX 7447

0.30

3

MG 2E (38%)

45.80

3

CONREZ (40%)

2.00

LAKEWAX 37

5.90

TOTAL

100.00

Fmln No 103C

HIGH GLOSS POLISH Ingredients

Weight Percent

WATER

33.78

DIETHYLENE GLYCOL MONOETHYL ETHYL

4.20

TRIBUTOXYETHYL PHOSPHATE

3.70

1

FLUORAD FC 129 (1% SOLUTION)

0.50

2

ABEX 18S

1.20

3

TEGO FOAMEX 7447

0.02

4

PROXEL GXL

0.10

5

MG 2E (38%)

49.40

5

MC 1030

1.00

LAKEWAX 37

3.10

LAKEWAX 57P

3.00

TOTAL

100.00

Fmln No 103D HIGH GLOSS, GOOD DURABILITY, LOW SLIP Ingredients

Weight Percent

WATER

38.3

DIETHYLENE GLYCOL MONOETHYL ETHER

6.5

TRIBUTOXYETHYL PHOSPHATE

2.5

FLUOROSURFACTANT (1% SOLUTION)

0.8

1

PROXEL GXL

0.1

2

MG 2E (38%)

40.5

2

CONREZ (40%)

1.9

TOTAL

LAKEWAX 52

10.5

LAKEWAX 37

1.7 100.0

Fmln No 103E TRANSLUCENT FLOOR POLISH Applied via sponge or cloth, gives high gloss. Ingredients WATER DIETHYLENE GLYCOL MONOETHYL ETHER TRIBUTOXYETHYL PHOSPHATE AMMONIUM HYDROXIDE (28%) FLOUROSURFACTANT (1% SOLUTION) 1

PROXEL GXL

Weight Percent 54.1 4.5 1.1 1.0 0.5 0.1

C9/11 alcohol + 6EO

1.0

2

MHL-100 (40%)

31.0

2

MC 1030

4.2

LAKEWAX 37

2.5

TOTAL

100.00

Fmln No 103F

FAST DRYING, GOOD RECOATABILITY Ingredients WATER DIETHYLENE GLYCOL MONOETHYL ETHYL TRIBUTOXYETHYL PHOSPHATE FLOUROSURFACTANT (1% SOLUTION)

1

Weight Percent 50.33 2.60 2.60 0.60 0.02

2

TEGO FOAMEX 7447

3

PROXEL GXL

0.10

4

ML870E LATEX (40%)

38.40

LAKEWAX 37

2.85

LAKEWAX 57P

2.50

TOTAL

100.00

Fmln No 103G MARBLE/TERRAZZO POLISHES 18% Solids

24% Solids

ITEM

WEIGHT%

ITEM

WEIGHT%

Water

54.51

Water

40.61

Diethylene Glycol

Diethylene Glycol

Monoethyl Ether

2.30

Monoethyl Ether

3.24

Tributoxyethyl Phosphate

2.30

Tributoxyethyl Phosphate

3.24

Fluorosurfactant (1% soln)

0.50

Fluorosurfactant (1% soln)

0.50

0.02

1

Tego Foamex 7447

0.02

0.10

2

Proxel GXL

0.10

ML-877E Latex (40%)

47.79

1 2

Tego Foamex 7447 Proxel GXL

ML-877E Latex (40%)

34.00

MC 1030 (30% soln)

2.27

Lakewax 37

2.00

Lakewax 37

2.50

Lakewax 57P

2.00

Lakewax 57P

2.00

TOTAL

100.00

TOTAL

100.00

Fmln No 103H

GOOD LEVELLING PROPERTIES, FAST RECOATABILITY Ingredients WATER DIETHYLENE GLYCOL MONOETHYL ETHYL TRIBUTOXYETHYL PHOSPHATE FLOURAD FC 129 (1% SOLUTION)

1

Weight Percent 50.28 2.80 2.80 0.50 0.10

2

PROXEL GXL

3

TEGO FOAMEX 7447

0.02

4

ML877E (40%)

41.50

LAKEWAX 37

2.00

TOTAL

100.00

Fmln No 103I

FORMULATIONS WITH GOOD LEVELLING, HIGH GLOSS, HARD WEARING Ingredients WATER DIETHYLENE GLYCOL MONOETHYL ETHER TRIBUTOXYETHYL PHOSPHATE SYNPERONIC 13/6.5

1

Weight Percent 48.72 2.85 2.60 0.20 0.10

2

PROXEL GXL

3

POLYFOX TM-1 (1% SOLUTION)

1.20

4

TEGO FOAMEX 7447

0.03

3

ML 878 (40%)

39.80

LAKEWAX 37

4.50

TOTAL

100.00

Fmln No 103J Ingredients WATER DIETHYLENE GLYCOL MONOETHYL ETHER TRIBUTOXYETHYL PHOSPHATE PROXEL GXL

1

Weight Percent 32.34 7.78 3.00 0.10 1.20

2

POLYFOX TM-1 (1% SOLUTION)

3

TEGO FOAMEX 7447

0.02

2

ML 878 (40%)

46.86

2

MC 3040

3.14

LAKEWAX 37

5.56

TOTAL

100.00

Fmln No 103K Ingredients WATER DIETHYLENE GLYCOL MONOETHYL ETHER TRIBUTOXYETHYL PHOSPHATE PROXEL GXL

1

Weight Percent 35.28 3.90 3.50 0.10 1.20

2

POLYFOX TM-1 (1% SOLUTION)

3

TEGO FOAMEX 7447

0.02

2

ML 878 (40%)

54.10

LAKEWAX 37

1.90

TOTAL

100.00

Fmln No 103L Ingredients WATER DIETHYLENE GLYCOL MONOETHYL ETHER TRIBUTOXYETHYL PHOSPHATE PROXEL GXL

1 2

POLYFOX TM-1 (1% SOLUTION)

3

TEGO FOAMEX 7447

2

2.00 0.10 1.20

50.70

LAKEWAX 37 TOTAL

32.08 8.00

0.02

ML 878 (40%)

LAKEWAX 57P

Weight Percent

3.10 2.80 100.00

STAINLESS STEEL CLEANER A

B

Raw Material Lakeland PA 100 Citric Acid Genapol XO 50 Genapol LRO Liquid Genapol PF 20 Perfume Balance Water

% Weight 7% 3% 0.2% 0.3% 0.2% 1.0%

Lakeland PA 100 Genapol XO 50 Genapol PF 20 Balance Water

10% 0.5% 0.2%

ALUMINIUM/STAINLESS STEEL CLEANER Raw Material Water Lakeland AMA LF40 Lakeland PA 100 Alcohol Ethoxylate (C13-15 + 9EO) Butyl Oxitol

% Weight 78.0% 5.0% 10.0% 2.0% 5.0%

Apply by spray or cloth neat

GEL HAND CLEANER BASED ON D’LIMONENE A

B

Raw Material D’Limonene Alcohol Ethoxylate C9-11 + 6 EO Oleic Acid Lakeland AMA-L

% Weight 25.6% 13.0% 7.1% 10.7%

Triethanolamine Water

3.6% 40.0%

First prepare “A” using above order of addition with stirring at 50°C. In a separate container prepare solution “B” and warm to 50°C. Add (B) to (A) with stirring at 50°C and pack-off whilst at 50°C (once cooled blending is not possible/very difficult). The above formulation produces a clear gel on cooling.

106. BIOCIDAL HARD SURFACE CLEANER Raw Material Lakeland AMA Benzylammonium Chloride (50%) C13/C15 Alcohol-ethoxylate, 7 mole NTA Solution (40%) Dipropyleneglycol-monomethyether or Butylethoxol

% Weight 5% 5% 3% 5% 3%

Water

79% 107

LOW FOAM RINSE AID FOR DOMESTIC AND INDUSTRIAL DISHWASHING

A

B

Raw Material Synperonic LFRA 290* Synperonic LFRA 30* Citric Acid Isopropanol Lakeland AMA LF 40

% Weight 6% 6% 5% 5% 3%

Synperonic LFRA 290* Synperonic LFRA 260* Citric Acid Isopropanol Lakeland AMA LF 40 Balance Water

10% 2% 5% 5% 5%

* Biodegradable Low Foam Alcoholalkoxylates

108 BEER BOTTLE LABEL REMOVER Ingredient

WT%

Water LAKELAND AMA LF40 Sodium Gluconate Sodium Hydroxide Pearl

75.00 1.50 1.00 22.50

APPLICATIONS High temperature soak-tank for removing paper labels and cleaning beverage containers RECOMMENDED DILUTIONS Dilute 1 part to 8 parts of water to give 2.8% NaOH. Use a temperature of 65EC (or higher) to clean bottles.

BOTTLE WASH FORMULATIONS Ingredient

WT%

Water LAKELAND AMA LF40 Potassium Hydroxide 50% Sodium Gluconate Low Foam Nonionic

80.5 2.0 11.0 5.0 1.5

Brewery Concentrate Wt% Ingredient Water Gluconic acid (50%) Citric acid Lakeland CS100LF

30.0 50.0 10.0 10.0

The above concentrate is added at a rate of 0.2% concentration to a 2% solution of sodium hydroxide

Brewery Liquid Wt% Ingredient LAKELAND PPE604 C12-15 +4EO alcohol ethoxylate Sodium Citrate Sodium Gluconate Sodium hydroxide Water

3.75 1.25 10.0 10.0 1.5 73.5

Materials should be blended at room temperature, to water in the order given.

FLOOR POLISH FORMULATIONS BASED ON LAKEWAX 20 109.A Wet Mop Floor Polish % Wt 30 48.5 0.5 1.0 2.0 3.0 15.0

RAW MATERIAL LAKEWAX 20 Water EDTA Na4 Ethyl Diglycol C13 alcohol + 8EO C13-18 sodium alkane sulphonate Iso-propanol

109.B Spray cleaners with Polish Effect % Wt 20.0 57.4 20.0 2.0 0.1 0.5

RAW MATERIAL LAKEWAX 20 Water White Spirit C13 alcohol + 8EO C13-18 sodium alkane sulphonate Fluoro surfactant (wetting agent)

109.C Wash and Wax (Vehicles) % Wt 5.0 86.5 6.0 0.5 2.0

RAW MATERIAL LAKEWAX 20 Water Lakeland AMA Imidazoline 18OH C13-15 alcohol + 9EO

ENGINE DEGREASER % Wt RAW MATERIAL 38.0 DDBSA, Monoisopropylamine salt 38.0 NP 5 4.0 IMIDAZOLINE 18OH 20.0 Shellsol S

The above formulation should be clear when diluted 10 parts with 90 parts diesel. A 5% dilution of the diesel solution in water should yield a stable emulsion.

SHOE POLISH FORMULATIONS LOW VISCOSITY FOR LEATHER CARE, SOLVENT FREE Water Kelzan S (1) Silicone oil Emulsion C13 alcohol + 5EO(2) Acrylic Polymer Dsipersion LAKEWAX 20 (1) (2)

56.6 0.1 20.0 0.3 3.0 20.0

Thickening agent, Kelco eg Genapol X 050, ex Hoechst

SELF SHINE POLISH FOR BOTTLE/SPONGE APPLICATION Water Ethanol Levelling/Wetting agent(1) Acrylic Polymer Dsipersion Tributoxyethylphosphate LAKEWAX A37D LAKEWAX 20 (1)

eg Licowet F3 1% solution, ex Hoechst

20.0 10.0 1.0 8.0 1.0 10.0 20.0

112 A. Formulation With Good Filling Power For Porous Floor-Coverings: % Weight

Material 50 LAKEWAX 20 5 Licomer A 53 Conc (1) 45 Water

Mix components in above order at room temperature (1)

Clariant

112 B. Mild Cleaning Solution for Waxed Floors: % Weight 3 5 5 87 (1)

Material LAKELAND AMA LF40 C 13/15 Alcohol + 6EO TKKP (50 % solution) (1) Water

Tetrapotassium pyrophosphate

113. LOW FOAM FLOOR CLEANER/WAX STRIPPER

% WEIGHT a.

10% 5% 3% 6% 1%

b.

5% 5% 4% 5% 4%

c

5.0% 1.0% 10.0% 12.0%

RAW MATERIAL Caflon KP50 (Tetrapotasium pyrophosphate 50%) Sodium Tripolyphosphate Sodium Metasilicate Lakeland AMA LF 40 or PPE 604K Ukanil 2357 (Low Foam Fattyalcoholalkoxylate) Balance Water Lakeland AMA LF 40 or AMA NTA Solution (40%) Ukanil 2357 (Low Foam Fattyalocholalkoxylate) Sodium Metasilicate Closol MP2 (Dipropyleneglycolmonoethylether) or Butylethoxol Balance Water LDP89(Lakeland development product) Sodium hydroxide Potassium silicate(50% solution) Tetra potassium pryophosphate Balance water

ALUMINIUM CLEANERS – ALKALI 114 A Soak Tank Cleaner/Brightner Raw Material Lakeland AMA LF40 KOH (50 %) EDTA powder Sodium silicate solution Alcohol Etoxylate (C9/11 + 5 – 10 EO) Water

% Weight 6 10 1 15 2 66

114 B Alkali Aluminium Brightner Raw Material Lakeland AMA LF40 KOH (50% solution) NaOH (32% solution) EDTA or NTA powder Alcohol Etoxylate (C9/11 + 5 – 10 EO) Water

% Weight 7 4 20 5 2 62

Train Cleaner-Oxalic Based

Raw Material Lakeland PPE 604 Water Oxalic Acid Orthophosphoric acid Alcohol Etoxylate (C9/11 + 6 EO) DDBSA

% Weight 1.5 56.0 4.5 20 8 10

116. NON – CAUSTIC STEAM CLEANER

% Wt 4 4 8 1 83

RAW MATERIAL LAKELAND AMA LF70 C9/11 alcohol + 6/8 EO Sodium Tripolyphosphate Sodium Metasilicate (5H2O) Water

LIQUID HAND SOAP Raw Material Sodium Lauryl Ether Sulphate Lakeland CAB or AMA-L Oleic Acid Water

% Weight 30 8 3 59

Citric acid can be added to adjust the pH. Also NaCl can be added to increase viscosity.

GLASS CLEANERS 118.A Glass Cleaner % Wt

RAW MATERIAL 2 LAKELAND AMA LF40 2 Acetic Acid 96 Water

118.B Ammoniated Glass Cleaner % Wt 2.5 0.5 2.5 94.5

RAW MATERIAL LAKELAND AMA LF40 EDTA Na4 Ammonia (880/890) Water

LAUNDRY CLEANERS 119.A & B Restaurant/Hotel Laundry % Wt A

RAW MATERIAL B

8 54 25 8 5

8 50 25 8 5 4

LAKELAND AMA LF40 Water KOH (50 % liquid) C9/11 alcohol + 6-8EO STPP Potassium Silicate

CREAM CLEANSERS 120.A Light Duty % Wt 10 10 2 3 0.5 74.5

RAW MATERIAL DDBSA, Na (25%)* Calcium Carbonate Sodium Carbonate Cocodiethanolamine AMA Water

120.B Heavy Duty % Wt 17.5 45 4 1 0.5 0.3 31.7

RAW MATERIAL DDBSA, Na (25%)* Calcium Carbonate Potassium Silicate C9/11 alcohol + 6 EO C9/11 alcohol + 3 EO AMA Water

Oven cleaners 121A Foaming type % Wt 1.5 1.0 2.5 5.0 90.0

RAW MATERIAL Lakeland AMA Ammonium lauryl sulphate (28%) Phenol +4EO Sodium hydroxide water 121.B Gel type

% Wt 0.7 0.3 10.0 2.0 87.0

RAW MATERIAL Veegum Xanthan Gum Sodium hydroxide 10.0 Lakeland PAE136 Water 121.C Thickened liquid

% Wt 1.0 15.0 0.5 83.5

RAW MATERIAL Xanthan Gum Sodium hydroxide LDP89 water

Metal cleaners, Immersion types 122 A Light duty for ferrous and non ferrous metals % Wt 4.00 1.20 0.65 13.60 80.55

RAW MATERIAL Lakeland PPE604 C13-C15 alcohol +4EO Sodium hydroxide TKPP Water

122B Medium duty for Ferrous and non ferrous metals % Wt 4.00 1.20 10.00 5.00 78.30

RAW MATERIAL Lakeland PPE604 C13-C15 alcohol +4EO Sodium Silicate NTA trisodiun salt Water

122.C Heavy Duty for ferrous metal % Wt 4.00 1.20 15.00 7.50 15.0 57.30

RAW MATERIAL Lakeland PPE604 C13-C15 alcohol +4EO Sodium hydroxide Sodium heptonate Sodium silicate Water 122D Low foam

% Wt 2.00 9.00 14.00 75.00

RAW MATERIAL LDP89 Potassium Hydroxide TKPP Water

Metal cleaners, Spray types 123 A High temperature system % Wt 7.00 7.00 7.50 5.00 73.5

RAW MATERIAL Sodium Hydroxide LAKELAND CS 100-LF Sodium heptonate NTA tri sodium salt WAter 123B Pretreatment

% Wt 1.50 5.00 5.00 5.00 10.0 73.5

RAW MATERIAL Sodium Hydroxide LAKELAND CS 100-LF TKPP NTA tri sodium salt Sodium silicate Water

Metal cleaners, Electrolytic 124A, Medium Foam % Wt 10.00 3.00 15.00 16.00 10.00 46.00

RAW MATERIAL Lakeland PPE604 C13-C15+8EO Sodium Hydroxide TKPP Potassium silicate Water 124B Low Foam

% Wt 13.00 15.00 16.00 10.00 46.00

RAW MATERIAL LDP89 Sodium hydroxide TKPP Potassium Silicate Water

Metal cleaners, Rinsing formulations 125A, Removal of silicates % Wt 5.0 20.0 5.0 70.00

RAW MATERIAL Sodium hexametaphosphate Ethylan TB345* Lakeland PPE604K Water

* Defoamer 125B General purpose low active rinse aid % Wt 1.00 2.00 5.00 1.00 91.0

RAW MATERIAL Alcohol alkoxylate Phenol +4EO Lakeland PPE604K Sodium hydroxide Water

126. Trailer Curtain Cleaner – Low Foam % Wt 5.0 3.0 6.0 5.0 7.0 3.5 70.5 1

RAW MATERIAL LAKELAND AMA LF40 LAKELAND CS100-LF Butyl Diglycol TKPP (50%) NTA Solution (38%) Sodium Hydroxide (32 %) Water

Carpet Cleaners 127A Foaming Cleaner, Hand Application % Wt 5.0 2.0 6.0 7.0 3.0 77.0

RAW MATERIAL LAKELAND AMA LAKELAND PAE 136 Lauryl Ether Sulphate (28%) Tetrapotassium Pyrophosphate (50%) C14 – C18 fatty acid 2-ethylhexylester Water

Low Foaming Carpet Cleaners 127B % Wt 6.0 2.0 8.0 6.0 4.0 2.0 72.0

RAW MATERIAL LAKELAND AMA LF40 LAKELAND PAE 802 Sodium Silicate (50%) Sodium Tripolyphosphate C14 – C18 fatty acid 2-ethylhexylester NTA Na3 (38%) Water

127C % Wt 6.0 3.5 2.0 2.0 6.0 80.5

RAW MATERIAL LAKELAND AMA LF40 Low foam non-ionic NTA Na3 (38%) Sodium metasilicate Sodium Tripolyphosphate Water

128A. Industrial Laundry Detergent % Wt 6.0 1.5 3.0 3.0 5.0 81.5

RAW MATERIAL LAKELAND AMA EDTA Na4 TKPP (50%) Sodium Metasilicate C9/11 + 6 EO Water

128B. Laundry Detergent, Hotels etc % Wt 8.0 12.0 5.0 5.0 5.0 81.5

RAW MATERIAL LAKELAND AMA LF40 KOH Flake STPP C9/11 + 6 EO Potassium Silicate Water

129. Machine Dishwash Products a. Liquid % Wt 5.00 10.00 3.00 3.00 79.0

RAW MATERIAL Sodium Gluconate Sodium Hydroxide EDTA, trisodium salt Lakeland CS100LF Water

b. Liquid concentrate

% Wt 1.5 0.5 15.00 5.00 16.00 62.00

RAW MATERIAL Sodium Gluconate Sodium metasilicate NTA, trisodium salt Lakeland CS100LF* Sodium hydroxide Water

* pre neutralise prior to addition

130. METAL WORKING A.

SEMI-SYNTHETIC FLUID (MICRO EMULSION) Water Paraffinic Oil Boric Acid Fatty Acid Lakeland PAE 185 Monoethanolamine

-

25.0% 20.0% 15.0% 15.0% 5.0% 20.0%

The above is a clear micro emulsion which can be diluted to 5% in water for use.

B.

SOLUBLE OIL Petroleum Sulphonate Lakeland PAE 185 Naphthenic Oil Rapeseed Oil Triethanolamine

-

20.0% 8.0% 62.0% 5.0% 5.0%

The above is a clear solution and when diluted forms milky emulsion.

C.

SYNTHETIC (AQUEOUS BASED) CUTTING FLUID Water Soluble Polyalkylene Glycol Lakeland PPE 604 Triethanolamine Lakeland AMA LF 40 Water

-

20.0% 10.0% 6.0% 20.0% 44.0%

The above is a clear and low foaming solution that is soluble in water in all proportions.

131. HEAVY DUTY DEGREASER - ALKALI

Raw Material Lakeland AMA or AMA LF40 KOH (50 %) EDTA powder Butyl Oxitol Alcohol Etoxylate (C9/11 + 8 – 10 EO) DDBSA Water

% Weight 8 20 4 3 2 1.5 61.5

132. INSECT REPELLANT HARD SURFACE CLEANER

Raw Material Lakeland AMA Alcohol Ethoxylate C9-11 + 6 EO

EDTA powder Merck Insect Repellent 3535 Perfume Citroder 56021 Perfume Alpin 560289 Dye Duramine Blue

Water

% Weight 7.000 4.000 4.000 3.000 0.200 0.200 0.002 85.598

The above product should be diluted 10 - 15 % and applied by cloth / mop during normal cleaning procedures.

133. ANTI-GRAFFITI COATING

Raw Material

% Weight

Water Ethyl Diglycol Tributoxyethyl Phosphate (1) Zonyl FSP (1% solution) Benzisothiazolone (biocide) (2) Morcryl MC-1030 (3) Morton ML-877E (40%)

40.86 0.84 0.36 0.48 0.10 5.95 12.45 30.96

Lakewax 37

The above should be applied neat by spray and allowed to dry. Removal of coating is accomplished using a mild alkaline cleaner through a pressure washer or using a volatile amine or ammonia solution. (1) (2) (3)

ex-Dupont ex Omnova Solutions, UK.

134. Formulation With Good Filling Properties For Porous/Wood Floors % Weight 50.0 5.0 5.0 0.2 39.8 (1)

Clariant

Material LAKEWAX 20 Licomer A 53 Conc (1) Butyl Oxitol Imidazoline 18OH Water

135. High Alkaline, Highly built, Low Foam Cleaner, for Dairy/Food Processing % Weight 6.0 20.0 15.0 59.0

Material LAKELAND CS100LF Sodium Hydroxide Prills EDTA Na4 Water

136. Aluminium Degreaser % Weight 4.5 2.0 10.0 4.5 4.0 75.0

Material LAKELAND LDP 80 LAKELAND AMA LF40 TKPP (50% solution) Sodium Metasilicate (5 H2O) C9/11 alcohol + 4/5 EO Water

137. Cleaner/Descaler, Light Duty % Weight 2.0 2.0 4.0 1.0 81.0

Material LAKELAND PA 100 LAKELAND AMA Citric acid C9/11 alcohol + 4/5 EO Water

138. Wheel Cleaner % Weight 2.0 2.0 0.3 30.0 1.0 64.7

Material LAKELAND PA 100 LAKELAND AMA LF40 IMIDAZOLINE 18OH HCl conc C9/11 alcohol + 4/5 EO Water

139 - Screenwash Formulation 0.6% Lakeland AMA LF40 5% IPA or butyl oxitol 0.2% DDBSA (Na Salt) Balance water Perfume and dye

This formulation is to be used as is, with no further dilution necessary.

Personal Care 140A Hand Cleaner % Wt

RAW MATERIAL 15 Lakeland CTA/N 30 Lauryl Ehter Sulphate (27%) Citric Acid, to pH 6.5 Sodium Chloride, to desired viscosity Balance Water

140.B Shower Gel % Wt

RAW MATERIAL 12 Lakeland CAB 25 Lauryl Ehter Sulphate (27%) Citric Acid, to pH 6.5 Sodium Chloride, to desired viscosity Balance Water

140.C Economical Hair Shampoo % Wt 9 25 3

Balance

RAW MATERIAL Lakeland CAB Lauryl Ehter Sulphate (27%) Coconut Diethanolamide Citric Acid, to pH 7.0 Sodium Chloride, to desired viscosity Water

140.D Foam Bath % Wt 12 20 3

Balance

RAW MATERIAL Lakeland CAB Lauryl Ehter Sulphate (27%) Coconut Diethanolamide Citric Acid, to pH 7.0 Sodium Chloride, to desired viscosity Water

Upholstery Cleaner Ref 141 % Wt

4.0 3.0 2.0 6.0 1.0 84.0

RAW MATERIAL LAKELAND AMA LF40 Sodium Metasilicate (5H2O) EDTA Na4 Butyl Oxitol Propan-2ol Water

Traffic Film Removers (Pressure Wash) Standard TFR 142.1

% Wt

5.0 5.0 4.0 2.0 2.0 0.6 81.4

RAW MATERIAL LAKELAND AMA Sodium Metasilicate (5H2O) NTA Na3 powder EDTA Na4 powder Alcohol Ethoxylate (C9-C11 + 6EO) Sodium Hydroxide Water

Neutral TFR 142.2

% Wt

3.5 2.3 5.0 4.0 2.0 2.0 0.3 80.9

RAW MATERIAL LAKELAND AMA PAE 136 Sodium Metasilicate (5H2O) NTA Na3 powder EDTA Na4 powder Alcohol Ethoxylate (C9-C11 + 6EO) Sodium Hydroxide Water

STEAM CLEANING Ref 143 Steam Cleaning concentrate

% Wt 16.0 15.0 10.0 3.75 1.25 54.0

RAW MATERIAL Tetra potassium pyrophosphate Potassium hydroxide Potassium silicate LAKELAND PPE604 C12-15 +4EO alcohol ethoxylate Water

Low foam steam concentrate % Wt 10.0 2.0 10.0 20.0 58.0

RAW MATERIAL LAKELAND CS100LF Sodium hydroxide Sodium metasilicate Tetrapotassium pyrophosphate Water

Materials should be blended at room temperature, to water in the order given

ABBATOIR CLEANERS Ref 144 Low Foam

% Wt 3.0 5.0 3.0 10.0 79.0

RAW MATERIAL LAKELAND CS100LF Sodium hydroxide prills EDTA tri sodium salt Sodium meta silicate water

Medium Foam % Wt 5.5 0.7 5.0 3.0 10.0 75.8

RAW MATERIAL LAKELAND PPE604K C9-11 +6EO alcohol ethoxylate Sodium hydroxide prills EDTA tri sodium salt Sodium metasilicate Water

% Wt 2.0 10.0 88.0

RAW MATERIAL LAKELAND AMA Sodium hydroxide Water

High foam

Materials should be blended at room temperature, to water in the order given

Low Foam Parts Cleaner (for machinery) 4% AMA LF40 10% Caustic 12% Metso 6% Sequestrant 4% nonionic 7% PAE 803K

LOW FOAM FLOOR CLEANER/WAX STRIPPER Ref 146

% Wt 6.0 6.0 0.2 2.0 85.8

RAW MATERIAL LAKELAND AMA LF40 Tetrapotassium Pyrophosphate Low Foam Alkoxylate Sodium meta silicate water

HIGH ACTIVE DISHWASHING LIQUID Ref 147

% Wt 10.0 11.7 47.3 26.0 5.0

RAW MATERIAL LAKELAND AMA Caustic Soda Solution (32%) Sodium Alkyl Ether Sulphate (27% Na salt) Alkyl Benzene Sulphonic Acid (Broad Cut) Coconut Diethanolamide

Add Sodium Alkyl Ether Sulphate to the Lakeland AMA stir until clear. Add the Caustic Soda solution with stirring followed by the Coconut Diethanolamide. Add the Alkyl Benzene Sulphonic Acid slowly with stirring. Heating may be required to improve viscosity and to eliminate trapped air in the product during manufacture. The pH of the product should be 6.5 - 7.5. This product can be diluted to desired activity, normally between 10 - 30%, and if required can be taken to desired viscosity by the addition of salt.

148. Heavy Duty Liquid Laundry Detergent

Water Tall Oil Fatty Acid Potassium Hydroxide (90%) Lakeland AMA Lakeland LF60 Lakeland PPE 604 NTA Na3 (38%) Tetrapotassium Pyrophosphate Alcohol Ethoxylate (C13-15,9 Mole EO) Lakeland PAE 802 Tinopal DMS/X

-

44.75% 4.85% 1.10% 15.00% 3.00% 1.00% 5.80% 14.00% 9.30% 1.00% 0.20%

Add TOFA to the water then the KOH and stir until homogeneous. Add the remaining RM’s in the above order (except Tinopal). Stir until homogeneous. Add the Tinopal with stirring until a clear fluorescent solution is obtained (heating to 40 oC may be necessary). The product should be used in automatic washing machine at dilution of 11-13 ml/L depending on water hardness.

Leather Care Treatments Low Viscosity, Self Shine Emulsion for bottles with Sponge Applicators 10% 30% 1% 50% 8% 1%

Ethanol Water, partly replaced by water soluble dyes or pigments are used for colouring Tributoxyethylphosphate (Plasticizer) Lakewax 20 Acrylic Polymer Dispersion Levelling / wetting agent

Fine Leather Care Products 47.4% 0.1% 24.7% 0.3% 2.5% 25%

Water Kelzan S Silicon Oil emulsion E10 Nonionic Emulsifier (Genapol X 050) Polymer Dispersion (Mowilith DM 772) Lakewax 20

Notes on the above formulations: Solvents are used in shoe polish formulations to aid cleaning. They dissolve soluble oil, particularly oily substances. Naphtha fractions such as white spirit / mineral spirits (140 – 200 oC) or more volatile boiling point spirits are preferred. The latter do not penetrate deeply into the leather and hence reduce the danger of staining sensitive leather. Ethanol is often used as a flow agent, antifoaming and wetting agent in aqueous care products. Plasticizers are used to improve wetting properties of liquid care products and the flexibility of the film after drying. Acrylic Polymer Dispersions improve water repellency and abrasion resistance. They should aid in producing a high gloss finish with excellent water resistance. Levelling / Wetting Agents are used for the fine tuning of low viscosity emulsions or aqueous leather finishes. 1-2% of a 1% fluorosurfactant solution are added. Kelzan S, a consistency regulatoris used to produce a heat stable shoe polish with a softer consistency. They are predispersed in water prior to the addition in the batch. Silicone oil dissolves in the solvent and is incorporated together with it since it cannot be homogeneously mixed with waxes. After solvent evaporation, it acts in the wax film as a lubricant and improves buffability without adversely affecting the other properties of the film. The water repellency of silicone oil is also an advantage.

150. Tile Cleaner % Weight 2.5 3.0 4.0 12.5 2.0 76.0

Material LAKELAND PA 100 LAKELAND AMA LF40 Sulphamic acid Phosphoric acid Low foam alcohol ethoxylate/Prop[oxylate Water

Aluminium Cleaners

151 A Light Duty, eg Bathrooms % Wt 1.00 1.00 2.00 2.50 0.50 1.50 92.00

RAW MATERIAL LAKELAND PA 100 LAKELAND AMA Propan-2-ol Citric acid C9/11 alcohol + 6EO Sodium Lauryl Ether Sulphate (3EO) Water

151 B Heavy Duty, eg Wheel Cleaning % Wt 5.00 0.10 0.50 5.00 10.00

RAW MATERIAL LAKELAND PA 100 IMIDAZOLINE 18OH C9/11 alcohol + 6EO Citric or Sulphamic acid Phosphoric acid Water

152. Plastic Cleaner

% Wt 2.00 5.00 0.30 1.00 91.70

RAW MATERIAL LAKELAND AMA LAKELAND PA800TEA C9/11 alcohol + 6EO Sodium Lauryl Ether Sulphate (3EO) Water